Revision of the McGraw-Hill textbook Modern Analytical Chemistry published in 1999. The new version includes practice exercises (with worked solutions), instructions on using Microsoft Excel and computational software, and method development and optimization.
Textbook is available as individual PDF files or a complete textbook in PDF form.
Each chapter concludes with a chapter summary, key terms, problems and solutions to the practice exercises.
Table of Contents for Analytical Chemistry Online Textbook
- Preface
- A. Organization
- B. Role of Equilibrium Chemistry
- C. Computational Software
- D. How to Use The Electronic Textbook’s Features
- E. Acknowledgments
- Introduction to Analytical Chemistry
- 1A. What is Analytical Chemistry?
- 1B. The Analytical Perspective
- 1C. Common Analytical Problems
- 1D. Key Terms
- Basic Tools of Analytical Chemistry
- 2A. Measurements in Analytical Chemistry
- 2B. Concentration
- 2C. Stoichiometric Calculations
- 2D. Basic Equipment
- 2E. Preparing Solutions
- 2F. Spreadsheets and Computational Software
- 2G. The Laboratory Notebook
- The Vocabulary of Analytical Chemistry
- 3A. Analysis, Determination and Measurement
- 3B. Techniques, Methods, Procedures and Protocols
- 3C. Classifying Analytical Techniques
- 3D. Selecting an Analytical Method
- 3E. Developing the Procedure
- 3F. Protocols
- 3G. The Importance of Analytical Methodology
- Evaluating Analytical Data
- 4A. Characterizing Measurements and Results
- 4B. Characterizing Experimental Errors
- 4C. Propagation of Uncertainty
- 4D. The Distribution of Measurements and Results
- 4E. Statistical Analysis of Data
- 4F. Statistical Methods for Normal Distributions
- 4G. Detection Limits
- 4H. Using Excel and R to Analyze Data
- Standardizing Analytical Methods
- 5A. Analytical Standards
- 5B. Calibrating the Signal (Stotal)
- 5C. Determining the Sensitivity (kA)
- 5D. Linear Regression and Calibration Curves
- 5E. Blank Corrections
- 5F. Using Excel and R for a Regression Analysis
- Equilibrium Chemistry
- 6A. Reversible Reactions and Chemical Equilibria
- 6B. Thermodynamics and Equilibrium Chemistry
- 6C. Manipulating Equilibrium Constants
- 6D. Equilibrium Constants for Chemical Reactions
- 6E. Le Chatelier’s Principle
- 6F. Ladder Diagrams
- 6G. Solving Equilibrium Problems
- 6H. Buffer Solutions
- 6I. Activity Effects
- 6J. Using Excel and R to Solve Equilibrium Problems
- 6K. Some Final Thoughts on Equilibrium Calculations
- Collecting and Preparing Samples
- 7A. The Importance of Sampling
- 7B. Designing A Sampling Plan
- 7C. Implementing the Sampling Plan
- 7D. Separating the Analyte from Interferents
- 7E. General Theory of Separation Efficiency
- 7F. Classifying Separation Techniques
- 7G. Liquid-Liquid Extractions
- 7H. Separation Versus Preconcentration
- Gravimetric Methods
- 8A. Overview of Gravimetric Methods
- 8B. Precipitation Gravimetry
- 8C. Volatization Gravimetry
- 8D. Particulate Gravimetry
- Titrimetric Methods
- 9A. Overview of Titrimetry
- 9B. Acid-Base Titrations
- 9C. Complexation Titrations
- 9D. Redox Titrations
- 9E. Precipitation Titrations
- Spectroscopic Methods
- 10A. Overview of Spectroscopy
- 10B. Spectroscopy Based on Absorption
- 10C. UV/Vis and IR Spectroscopy
- 10D. Atomic Absorption Spectroscopy
- 10E. Emission Spectroscopy
- 10F. Photoluminescence Spectroscopy
- 10G. Atomic Emission Spectroscopy
- 10H. Spectroscopy Based on Scattering
- Electrochemical Methods
- 11A. Overvier of Electrochemistry
- 11B. Potentiometric Methods
- 11C. Coulometric Methods
- 11D. Voltammetric Methods
- Chromatographic and Electrophoretic Methods
- 12A. Overview of Analytical Separations
- 12B. General Theory of Column Chromatography
- 12C. Optimizing Chromatographic Separations
- 12D. Gas Chromatography
- 12E. High-Performance Liquid Chromatography
- 12F. Other Forms of Liquid Chromatography
- 12G. Electrophoresis
- Kinetic Methods
- 13A. Kinetic Methods Versus Equilibrium Methods
- 13B. Chemical Kinetics
- 13C. Radiochemistry
- 13D. Flow Injection Analysis
- Developing a Standard Method
- 14A. Optimizing the Experimental Procedure
- 14B. Verifying the Method
- 14C. Validating the Method as a Standard Method
- 14D. Using Excel and R for an Analysis of Variance
- Quality Assurance
- 15A. The Analytical Perspective – Revisited
- 15B. Quality Control
- 15C. Quality Assessment
- 15D. Evaluating Quality Assurance Data
- Additional Resources
- Appendix
View this Free Online Material at the source:
Analytical Chemistry 2.0
